We need some more specifics. I would do a 40% water change (if it is a very small pond I would do more of a water change if it is over 10000 gallons less). Either way after the water change with dechlor added, an ammonia binder is a must until you figure out what it going on.
Tell us about the filtration that is on the pond and pond size. What is the pH of the source water and the kH readings. With pH that low a pH crash could occur and kill everything in the pond soon. If source water and kH readings are low you will need to buffer the water with something. Some use baking soda and I would think this would be better than doing nothing, but your source water will give more clues to the final deposition on this. What is the water temp?
Need more info,Aquitori.